synthesis and charaterization of magensium oxide mesoporous microstructures using pluronic f127

نویسندگان

a. tadjarodi

m. sedghi

k. bijanzad

چکیده

mesoporous  mgo  microstructures  were  synthesized  using magnesium  acetate  tetrahydrate,  ammonium  oxalate  monohydrate and  pluronic  f127  via  heating  at  40  °c  for  24  h  and  subsequent calcination. the mesoporous structure of magnesium oxide with the specific  surface  area  of  47m2/g,  pore  volume  0.30  cm3/g  and  the average pore size 24 nm is produced. according to xrd studies, the diffraction peaks of  the product pattern can be  indexed  to  the cubic structure magnesium oxide with  the  lattice parameter of a = 4.22 å and  showing  no  impurities.  the  product  was  characterized  by fourier  transform  infrared  spectroscopy,  x-ray  powder  diffraction analysis,  n2  adsorption-desorption  and  scanning  electron microscopy.

برای دانلود باید عضویت طلایی داشته باشید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Synthesis and Charaterization of Magensium Oxide Mesoporous Microstructures Using Pluronic F127

Mesoporous  MgO  microstructures  were  synthesized  using magnesium  acetate  tetrahydrate,  ammonium  oxalate  monohydrate and  Pluronic  F127  via  heating  at  40  °C  for  24  h  and  subsequent calcination. The mesoporous structure of magnesium oxide with the specific  surface  area  of  47m2 /g,  pore  volume  0.30  cm3 /g  and  the average pore size 24 nm is produced. According to ...

متن کامل

synthesis of amido alkylnaphthols using nano-magnetic particles and surfactants

we used dbsa and nano-magnetic for the synthesis of amido alkylnaphtols.

15 صفحه اول

Phase transfer of highly monodisperse iron oxide nanocrystals with Pluronic F127 for biomedical applications

Iron oxide nanoparticles made from the thermal decomposition method are highly uniform in all respects (size, shape, composition and crystallography), making them ideal candidates for many bioapplications. The surfactant coating on the as-synthesized nanoparticles renders the nanoparticles insoluble in aqueous solutions. For biological applications nanoparticles must be water soluble. Here we d...

متن کامل

Redox-sensitive Pluronic F127-tocopherol micelles: synthesis, characterization, and cytotoxicity evaluation

Pluronic F127 (F127), an amphiphilic triblock copolymer, has been shown to have significant potential for drug delivery, as it is able to incorporate hydrophobic drugs and self-assemble into nanosize micelles. However, it suffers from dissociation upon dilution owing to the relatively high critical micelle concentration and lack of stimuli-responsive behavior. Here, we synthesized the α-tocophe...

متن کامل

single-step synthesis of multi-component spirobarbiturates using ionic liquids and synthesis of substituted pyridine filled with catalysts supported on solid substrate

in this thesis, a better reaction conditions for the synthesis of spirobarbiturates catalyzed by task-specific ionic liquid (2-hydroxy-n-(2-hydroxyethyl)-n,n-dimethylethanaminium formate), calcium hypochlorite ca(ocl)2 or n-bromosuccinimide (nbs) in the presence of water at room temperature by ultrasonic technique is provided. the design and synthesis of spirocycles is a challenging task becaus...

15 صفحه اول

Peptide mapping by capillary electrophoresis with Pluronic F127.

Separation of peptides and proteins by capillary zone electrophoresis suffers from the interaction of these solutes with the capillary wall which results in the formation of broad peaks and low resolution. To minimize the protein/peptide-capillary wall interaction we tried to use Pluronic F127, a triblock copolymer of the general formula (polyethylene oxide)(x)(polypropylene oxide)(y)(polyethyl...

متن کامل

منابع من

با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید


عنوان ژورنال:
journal of nanostructures

ناشر: university of kashan

ISSN 2251-7871

دوره 2

شماره 3 2012

کلمات کلیدی

میزبانی شده توسط پلتفرم ابری doprax.com

copyright © 2015-2023